New applications of boron-doped diamond electrode for voltammetric determination of ascorbic acid

Ilona Sadok, Katarzyna Tyszczuk-Rotko, Agnieszka Szwagierek

Abstract


An unmodified boron-doped diamond electrode was used for the voltammetric determination of ascorbic acid (AA). The measurements were carried out in an acetate buffer solution of pH = 4.6 by differential pulse voltammetry (DPV). Under the optimized experimental conditions, AA gaves linear response in a broad concentration range from 5 · 10–7 to 2· 10–3 mol/dm3. The detection limit was 1.63 · 10–7 mol/dm3. The proposed procedure was applied for simple and fast voltammetric determination of ascorbic acid in human urine samples and commercially available dietary supplements.

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DOI: http://dx.doi.org/10.17951/aa.2015.70.2.13
Date of publication: 2016-02-15 12:20:02
Date of submission: 2016-02-15 10:30:26


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Copyright (c) 2016 Ilona Sadok, Katarzyna Tyszczuk-Rotko, Agnieszka Szwagierek